James,
Half a day or overnight, something this size doesn't suffer if left in too long, I have often forgotten bits and 2 or 3 days later they come out just the same as 1/2 a day.
I have a plastic square 5 gallon container on it's side with ones side cut out and an old Ikea tub as a lid and this just stands outside all the while.
I set this up because I make division plates as probably many know from posts I have made. These are all different sizes and thickness's and are laser cut in bulk. The best material to use is pickled and oiled steel but I don't often have a choice of material depending on what deal the laser cutters have made, remember they buy in tonnage.
So mostly I get laser commercial quality which has a hard shiny black oxide surface as it good for the laser, splatter doesn't stick and it's not reflective and because they can run at higher feed rates it's cheaper.
My problem is the small drills I use 2mm to 1/8" depending on model of plate suffer and suffer badly, that oxide is hard to get thru and the drill web degrades at an alarming rate leading to broken drills and crooked holes so that oxide has to go.
Tried all things, many work but costly in either £££ or time, surface grinding is slow and clogs the wheel up and these are £90 a pop. Send them out for Lumsden grinding and it's expensive on cost and time.
So an overnight in this solution, mixed up 1:3 or 1:4 with water fetches the scale off and you get a pristine plate with, I won't say no drill problems because I could right an article on drill life but not everyone has to drill over 20,000 holes in a day, or rather thier CNC has to drill them
This plate has done about 2 hours in reasonable new solution but really needs a bit more but if pushed that scale that's left is loose and will scotchbrite off but a couple more hours and everything washes off with a hosepipe.
When the solution is used up you can empty it down the drain and before some H&S Nazi gets on my case it's sold for this exact purpose, brush on the patio and hose off. When I throw it away though it's just dead dirty water.
Last year when I was sorting an old shed out ready to pull it down I found a builders bucket with some tools in it full of water where the roof had been leaking. These had been in there for 8 or 10 years and I was going to skip them but decided to see how good they would clean up.
I think they are a bit far gone ?
Anyway a full day in the tank and got this.
The drill actually worked without any oil on it. It won't replace missing metal eaten away by the rust but it will remove the rust..
I have read that you can do the same by electrolysis and washing soda with good results but just a tank you drop stuff in works for me with no faffing about.