So I finally got around to having another go at shimming the column.
I could only find one supplier of pre-cut shims for this size in the UK, and it was going to cost about £60 for the selection I wanted. Needless to say I cut my own shims, marking them as suggested.
I also ended up removing the column (as part of an unsuccessful attempt to rectify the dire backlash issues I'm having), and took the opportunity to lightly file the edges of the mating surfaces to remove any burrs, thoroughly inspected everything, and removed any imperfections. I then cleaned everything and re-assembled.
After three attempts with the new shims, over four points on the bed, I'm getting a maximum error of 0.001" over just over a 5" diameter (which is the largest continuous diameter I can get on the x-axis bed).
Is it worth chasing the 0.001", or do I leave it?
By the way, as before, three of the bolts needed shimming, and they were all different values., but it seemed much easier to get a result this time in terms of the shims corresponding to level corrections. I wonder if fettling the faces made a difference?
Any advice appreciated. Thanks.