Hi Peter,
A quick run down on the process is a s follows: –
1. Pack all your components in suitable a container with at leat 1/2″ of charcoal between them
2. Heat to 900deg C and hold at this temp for the requiered time–pentration is .005″ per hour so you need 4 hours for a .020″ case. Is it duering this time the grain growth occurs in the core due to being at an elevated temp for a long period
3. To resolve this–allow to cool–still in the box
4. reheat to the upper critical temp for the core, 830deg C–assuming the core is .02%C and quench in oil–you will now have a tough refined core and a hard but coarse grain case
5. Now heat again to the upper critical temp for the case–720deg C [case will be .09%C] and quench–this will give you a very hard and fine grain case.
6. Temper to your required hardness or just stress releive at say 150degC then finish by grinding polishing etc.
This is a quick run down on the prefered process but if you don’t need a thick case to allow for finishing you can cut corners and not fefine the case–grain growth will be less or minimal if you are producing only a .005″ case for instance. There is a lot more to the tech side [some a bit misty now] but this works well.
If my memory is good we used a set of books called Chapmans Workshop Practice some 40+ years ago at Tech School which had a lot of info regarding the above and Im sure there are more books available.
Good luck! Regards John.
PS if you want to speak to me please snd me your phone number
Edited By Stephen John Fawcett on 01/11/2009 11:36:25