Looking on line it was clear many people don't dry the plaster properly. I did two hours at very low, then ramped it up for another two hours, then ran flat out for about 20 minutes, it was then possible to pour out about half the PLA.
I used natural pure;y by chance
This was the result of a trial run, don't ask how it turned into aluminium bronze… the base is 10mm square.
A second run produced four from a single mould, one with a minor fault, one short of metal as I put a bit too much in the first two holes!
The two good ones are great for what I need, much better than I could fabricate something an inch high in about six parts (I'm no jeweller!). Patterns were printed at 0.025mm layer height, practical with such tiny prints and gives an excellent finish. The dimples are to guide drilling.